مشخصات پژوهش

صفحه نخست /Immobilization of Pd(0) ...
عنوان Immobilization of Pd(0) complex on the surface of SBA-15: A reusable catalyst for the synthesis of 5-substituted tetrazoles, sulfides and sulfoxides
نوع پژوهش مقاله چاپ‌شده در مجلات علمی
کلیدواژه‌ها SBA-15 Palladium Sulfide Sulfoxide 5-Substituted tetrazol
چکیده A simple and efficient method for the synthesis of 5-substituted tetrazoles, sulfides and sulfoxides in the presence of Pd(0) complex immobilized on mesoporous SBA-15 as an efficient, recoverable and thermally stable mesostructure has been reported. Also, the prepared mesostructure was characterized by Fourier transform infrared spectroscopy, scanning electron microscopy, X-ray mapping, energy-dispersive X-ray spectroscopy, N2 adsorption and desorption, inductively coupled plasma optical emission spectroscopy and thermal gravimetric analysis. Then, this mesostructured catalyst was applied in the synthesis of 5- substituted tetrazoles, sulfides and sulfoxides. The approach described here offers advantages such as short reaction times, high yield, purity yields, simple and eco- friendly, easy work-up. More importantly, this nanohybrid robust catalyst did not undergo metal leaching and applied several times without any decrease in catalytic activity
پژوهشگران محمد قادرمزی (نفر سوم)، آرش قربانی چقامارانی (نفر دوم)، طیبه تامرادی (نفر اول)