عنوان
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Synthesis of a new Pd(0)-complex supported on magnetic nanoparticles and study of its catalytic activity for Suzuki and Stille reactions and synthesis of 2,3-dihydroquinazolin-4(1H)-one derivatives
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نوع پژوهش
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مقاله چاپشده در مجلات علمی
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کلیدواژهها
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Magnetic nanoparticle Palladium 2,3-Dihydroquinazolin-4(1H)-one Suzuki Stille
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چکیده
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In the present work, we report synthesis of anchored palladium complex on functionalized Fe3O4 nanoparticles via simple and inexpensive procedure. The final nanohybrid compound was characterized by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), energy-dispersive X-ray spectroscopy (EDS), inductively coupled plasma optical emission spectroscopy (ICP-OES), Xray Diffraction (XRD), thermal gravimetric analysis (TGA) and vibrating sample magnetometer (VSM) measurements. The catalytic activity of Fe3O4-Serine-Pd as an efficient and reusable catalyst was investigated for Suzuki and Stille reactions and synthesis of 2,3-dihydroquinazolin-4(1H)-one derivatives. The heterogeneous catalyst could be easily separated by applying a simple magnet and reused several consecutive runs without appreciable change in its catalytic activity
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پژوهشگران
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محمد قادرمزی (نفر سوم)، آرش قربانی چقامارانی (نفر دوم)، طیبه تامرادی (نفر اول)
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